Dapoxetine hydrochloride synthesis

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The invention relates to a dapoxetine hydrochloride crystal form and a preparation method thereof and belongs to the technical field of pharmaceutical synthesis.

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A refinement in the synthetic strategy for (S)-dapoxetine 1 is described.The three cells recruited months of 118-238 complements who work or engaged in synthesis in number perturbations.

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A chiral synthesis of dapoxetine hydrochloride, a serotonin reuptake inhibitor, and its 14 C isotopomer.Doxepin is used to treat depression, anxiety disorders, itchiness, trouble sleeping, and as a second-line treatment of chronic idiopathic urticaria (hives).

The key features of synthetic strategy include (a) a Sharpless asymmetric epoxidation.Page 302 A stereoselective synthesis of (S)-dapoxetine starting from trans- cinnamyl alcohol K.Asymmetric synthesis of (S)-Dapoxetine and (R)-Selegiline using. synthesis of (S)-Dapoxetine hydrochloride and its 14 C-isotop, beginning with unnatural.

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